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PRODUCTION OF TANTALUM HYDRATE AND/OR NIOBIUM OXIDE AND RESULTED TANTALATE AND NIOBATE

机译:氢氧化钽和/或氧化铌的生产以及所得的钽酸盐和铌酸盐

摘要

PURPOSE: To obtain spherical Ta and/or Nb oxide by adding an ammonia soln. contg. CO2 to an acidic fluoride soln. prepd. by dissolving Ta and/or Nb. ;CONSTITUTION: The ammonia soln. contg. the CO2 is added to the acidic fluoride soln. prepd. by dissolving the Ta and/or Nb until the pH thereof attains 7 and thereafter, the precipitate formed by reaction is filtered, by which the (hydrated) spherical Ta and/or Nb oxide is obtd. The (hydrated) spherical Ta and/or Nb oxide and the material selected from metal oxide, hydroxide and carbonate are mixed at a corresponding to stoichiometric ratio and the mixture is fired, by which the spherical tantalic acid and/or niobium acid metal having a BET value of 1 m2/g is obtd.;COPYRIGHT: (C)1996,JPO
机译:目的:通过添加氨溶液获得球形的Ta和/或Nb氧化物。续CO 2 转化为酸性氟化物溶液。准备通过溶解Ta和/或Nb。 ;组成:氨水。续将CO 2 添加到酸性氟化物溶液中。准备通过溶解Ta和/或Nb直至其pH达到7,然后过滤反应形成的沉淀,由此除去(水合的)球形Ta和/或Nb氧化物。以化学计量比将(水合的)球形Ta和/或Nb氧化物与选自金属氧化物,氢氧化物和碳酸盐的材料混合并烧制该混合物,从而使球形钽酸和/或铌酸金属具有<1 m 2 / g的BET值不变。;版权:(C)1996,JPO

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