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PROCESS FOR PREPARING ALKALINE AMINOBOROHYDRIDES AND ALKALINE AMINOBOROHYDRIDE COMPLEXES
PROCESS FOR PREPARING ALKALINE AMINOBOROHYDRIDES AND ALKALINE AMINOBOROHYDRIDE COMPLEXES
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机译:制备碱金属氨基硼酸盐和碱金属氨基硼酸盐复合物的方法
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摘要
A process is disclosed for preparing alkaline aminoborohydrides and alkaline aminoborohydride complexes by reacting a compound having the formula R?1R2NH.BH¿3 with an alkaline metal or amide in a solvent. A non-polar aliphatic or aromatic solvent and/or a bipolar aprotic solvent are used as solvents. The residues R?1 and R2¿ may be hydrogen or aliphatic, cycloaliphatic or aromatic residues. The end products obtained by this process have the general formulas M(R1R2N.BH3) or M(R1R2N.BH3).xL, in which L stands for the bipolar aprotic solvent, x for a numerical value from 0.1 to 5 and M for the alkaline metal.
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机译:公开了一种通过使式为R 1 R 2 NH.BH 3的化合物与碱金属或酰胺在溶剂中反应来制备碱性氨基硼氢化物和碱性氨基硼氢化物配合物的方法。非极性脂族或芳族溶剂和/或双极性非质子溶剂用作溶剂。 R 1和R 2残基可以是氢或脂族,脂环族或芳族残基。通过此方法制得的最终产物的通式为M(R1R2N.BH3)或M(R1R2N.BH3).xL,其中L代表双极性非质子溶剂,x代表数值0.1至5,M代表碱金属。
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