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Transversely heated tubular atomizing furnace

机译:横向加热管式雾化炉

摘要

The invention relates to a carbon-material, transversely or longitudinally heated atomising furnace (1) for flameless atomic absorption spectrometry and comprising a tube furnace section (17) and a sample carrier (2) in said tube furnace section. The improvement of the invention is that the sample carrier for fixing in the tube furnace has a central peg or foot (4) which is on the lower surface of said sample carrier and is fixed in a recess which corresponds substantially to the pegform, is in the centre of the inner wall of the tube furnace and substantially opposite the sample input opening. The sample carrier and the tube furnace section consist of electrographite. The gas-accessible surface of the sample carrier and the tube furnace section is coated with pyrocarbon. The two aforementioned parts are undetachably connected to each other in a defined manner by said pyrocarbon coating. The sample carrier preferably extends across the largest possible part of the longitudinal extension of the tube furnace. The surface of the sample carrier has a trough-shaped recess (5) which can hold up to a quantity of 50 mu l of analyte solution. The weight of the sample carrier is reduced by structural measures. When functioning, the atomising furnace demonstrates a good level of long-term stability with respect to sensitivity and reproducibility, and a larger linear concentration working range in relation to time-integrated extinction.
机译:本发明涉及一种用于无焰原子吸收光谱法的碳材料的横向或纵向加热的雾化炉(1),其包括管式炉段(17)和在所述管式炉段中的样品载体(2)。本发明的改进在于,用于固定在管式炉中的样品载体具有中心钉或脚(4),该中心钉或脚位于所述样品载体的下表面上并且固定在基本上对应于钉形的凹槽中。管式炉内壁的中心,基本上与样品输入口相对。样品载体和管式炉部分由电石墨组成。样品载体和管式炉的可通气表面涂有热碳。前述的两个部分通过所述热碳涂层以限定的方式彼此不可拆卸地连接。样品载体优选地延伸跨越管式炉的纵向延伸的最大可能部分。样品载体的表面有一个槽形的凹槽(5),可容纳多达50毫升的分析物溶液。通过结构措施减轻了样品载体的重量。运行时,雾化炉在灵敏度和可再现性方面显示出良好的长期稳定性,并且在时间积分消光方面显示出更大的线性浓度工作范围。

著录项

  • 公开/公告号DE29612065U1

    专利类型

  • 公开/公告日1996-09-12

    原文格式PDF

  • 申请/专利权人 ANALYTIK JENA GMBH 07745 JENA DE;

    申请/专利号DE1996212065U

  • 发明设计人

    申请日1996-07-11

  • 分类号G01N21/74;

  • 国家 DE

  • 入库时间 2022-08-22 03:42:44

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