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METHOD OF DETERMINATION OF GYROMAGNETIC RELATION OF NUCLEI

机译:核素核磁关系的测定方法

摘要

FIELD: study of structure of chemical compounds. SUBSTANCE: method includes acting on specimen of two HF pulses with time interval τ from beginning of cycle to beginning of the second pulse, setting of normal excitation conditions and registration of spin echo, calibrated measurement of value of HF field by the known specimen and determination of gyromagnetic relation of nuclei of tested sample. First pulse width is smoothly varied together with time interval for same value, modulation of echo signal is registered, frequency w1 is found by maxima of echo signals, and gyromagnetic relation of nuclei is determined as relation between this frequency ω1 and value of calibrating multifrequency field H1. EFFECT: higher efficiency. 2 dwg
机译:领域:研究化合物的结构。实质:该方法包括对两个HF脉冲的样本进行操作,样本间隔从周期开始到第二个脉冲开始的时间间隔为τ,设置正常激发条件并记录自旋回波,通过已知样本对HF场的值进行校准测量并确定样品核的旋磁关系对于相同的值,第一脉冲宽度随时间间隔平稳变化,记录回波信号的调制,通过回波信号的最大值找到频率w 1 ,并确定核的旋磁关系作为两者之间的关系ω 1 的频率和校准多频场H 1 的值。效果:更高的效率。 2 dwg

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