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Method and apparatus for NMR spectroscopy of nanoliter volume samples
Method and apparatus for NMR spectroscopy of nanoliter volume samples
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机译:用于纳升体积样品的NMR光谱学的方法和设备
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摘要
A method and apparatus for structural elucidation and determination of a nanoliter size sample of analyte. The method includes separating the analyte using a microseparation technique and then substantially simultaneously analyzing or detecting the sample using a nuclear magnetic resonance (NMR) spectrometer. The apparatus includes an RF microcoil positioned for operable communication with a capillary member of the microseparation system and the NMR spectrometer to provide enhanced sensitivity and improved signal-to-noise ratio of the NMR spectrometer necessary to accurately analyze or detect nanoliter size samples.
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