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A process for the preparation of hydroxyapatite powders for applications such as in bioceramics
A process for the preparation of hydroxyapatite powders for applications such as in bioceramics
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机译:制备用于例如生物陶瓷的羟基磷灰石粉末的方法
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摘要
A process for the preparation of hydroxyapatite powders for applications such as in bioceramics comprising in the steps of : a. dissolving a calcium salt such as .Ca (NO3) 2 in a solvent fol lowed by the addition of ammonia to form a first solution; b. dissolving a phosphate salt such as NH4H2PO4 in a solvent and adding ammonia to form a second solution; c. forming a gelatinous precipiate by adding said first solution at a temperature of 80-100oC to said second solution; d. subjecting said gelatinous precipiate to the. step of stirring for about 24 hrs.; .e. filtering and-washing said genatinous precipitate; f. subjecting said filtered and washed gelatinous precipitate to the step of freeze drying to obtain the hydroxyapatite powders.
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机译:一种用于例如在生物陶瓷中的应用的羟基磷灰石粉末的制备方法,包括以下步骤:a。将钙盐例如.Ca(NO 3)2溶解在通过添加氨而形成的第一溶液中的溶剂中; b。将诸如NH 4 H 2 PO 4的磷酸盐溶解在溶剂中,并添加氨以形成第二溶液。 C。通过在80-100oC的温度下向所述第二溶液中加入所述第一溶液形成凝胶状沉淀; d。使所述凝胶状沉淀物经受。搅拌约24小时的步骤; .e。过滤和洗涤所述植物沉淀。 F。使所述过滤并洗涤的凝胶状沉淀物进行冷冻干燥的步骤以获得羟基磷灰石粉末。
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