south korea from the peel and the risk for alcohol - extraction and separation of limonene

摘要

this invention is in recent years, breast cancer, colorectal cancer, pancreatic cancer, lung cancer and other cancer care about zero, together with risk for alcohol (perillyl alcohol) and d - limonene (d - limonene) peel from south korea for extraction and separation and purification of project management. the use of orange peel by using hexane extraction of fair use, the separation of the distribution process, the glass column was used, the risk of alcohol is the process and the use of liquid chromatography to the separation and purification of alcohol to the process composed of. taking the project of 100 u3396, pure ethanol in orange peel powder 5g in 50 ~ 55 degrees in order to maintain the temperature in the mixer in the mixing and pumping more than 3 hours.after the extract / hexane (1 / 5, volume ratio) is the ratio of mixed in a mixer for 30 minutes after the mixing of the powder into the funnel.;the separation of the ethanol and hexane layer by layer from the respective risk to alcohol and d - limonene and inclusion in the distribution. risk for alcohol contains ethanol extract of C18 filling the glass column filled with pure ethanol is used, the concentration of alcohol was to be. the method for the treatment of liquid chromatography in the amount of the water. the night time, the use of ethanol to move to move to, and the flow rate of 0.5 ~ 1 u3396 / min, UV shut the 205 nm as fixed and the sample analysis of the 10u3395 u03bc - Bondapak (3.9 x 300 mm 10 u339b) column, when the alcohol into risk analysis. and the risk for alcohol and d - limonene to commercial scale expansion, in order to analysis the issue from the same conditions as the specimen 10, 50, 100 u3395 15 u339b of C18 filler for filling can be used in manufacturing cylinder (3).9 x 300 mm), was injected into the alcohol will be drunk people.