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METHOD OF MANUFACTURING LEAD-ALUMINOSILICATE GLASS BY SOL-GEL METHOD

机译:溶胶-凝胶法制备铅铝硅酸盐玻璃的方法

摘要

The present invention relates to a method for producing lead aluminosilicate glass which can be used for semiconductor surface protection by the sol-gel method.;In the method for producing lead aluminosilicate glass using the sol-gel method of the present invention, a lead-based raw material, an aluminum-based raw material and deionized water are mixed and stirred to dilute a mixed aqueous solution and a silicon-based raw material to alcohols to form an alkoxide solution, respectively. Step 1; Stirring and mixing the alkoxide solution with stirring the mixed aqueous solution, followed by two steps of pouring ammonia water to react; Three steps of stirring until the treatment is uniform; Leaving the treated material to precipitate and then removing the clear solution at the top to obtain a glass gel solution; And it comprises a five steps of drying the glass gel solution, heat drying in an oxygen atmosphere.;According to this method, lead aluminosilicate-based glass for semiconductor bonding protection can be produced economically high purity and finer than conventional commercial glass powder.
机译:本发明涉及一种可通过溶胶-凝胶法用于半导体表面保护的铝硅酸铅玻璃的制备方法。在本发明的使用溶胶-凝胶法的铝硅酸铅玻璃制备方法中,将铝基原料和去离子水混合并搅拌,以将混合的水溶液和硅基原料分别稀释成醇以形成醇盐溶液。第1步;在搅拌混合的水溶液的同时搅拌并混合醇盐溶液,然后分两步倒入氨水以进行反应;搅拌三步直至处理均匀;留下处理过的物质沉淀,然后在顶部除去透明溶液,得到玻璃凝胶溶液。并且它包括干燥玻璃凝胶溶液,在氧气气氛中加热干燥的五个步骤。根据这种方法,可以经济地生产出纯度高,比常规市售玻璃粉末更细的用于半导体键合保护的铝硅酸铅基玻璃。

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