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METHOD FOR CORRECTING DEVIATION OF SPECTRAL ENERGY AXIS AT IDENTIFICATION FOR ANALYSIS ELEMENT

机译:用于确定分析元素的光谱能量轴偏差的校正方法

摘要

PROBLEM TO BE SOLVED: To highly accurately and automatically correct a deviation by carrying out an inner product process to each characteristic vector obtained by a predetermined process to measured spectral data and each candidate element data, and selecting an element to be axis-matched from candidate elements based on the process result.;SOLUTION: For example, in order to correct a deviation of a spectral energy axis in identifying elements of a sample surface by an electron probe microanalyzer, first, a peak is detected from measured spectral data with use of a secondary differentiation process or the like and candidate elements are selected in a predetermined method. Each data is normalized with use of a height of a maximum peak. A characteristic vector as a relative intensity to a position of the peak is formed. Peaks of the characteristic vectors are formed in a trapezoid to enable comparison even when the peaks deviate in position. Characteristic vectors of the spectral data and candidate element data are compared, and an inner product of the characteristic vectors is obtained by a predetermined method. An element which has a maximum value of the inner product is selected as an object to be axis-matched.;COPYRIGHT: (C)2000,JPO
机译:解决的问题:通过对通过预定处理获得的每个特征矢量执行内积处理,以对测量的光谱数据和每个候选元素数据进行内积处理,并从候选对象中选择要进行轴匹配的元素,以高度准确,自动地校正偏差解决方案:例如,为了校正通过电子探针微分析仪识别样品表面元素时光谱能轴的偏差,首先,使用质谱仪从测得的光谱数据中检测出一个峰二次微分处理等,并以预定方法选择候选元素。使用最大峰高对每个数据进行归一化。形成作为相对于峰的位置的相对强度的特征矢量。特征矢量的峰形成为梯形,即使在峰偏离位置时也能够进行比较。比较光谱数据和候选元素数据的特征向量,并且通过预定方法获得特征向量的内积。选择一个具有内积最大值的元素作为要进行轴匹配的对象。;版权:(C)2000,JPO

著录项

  • 公开/公告号JP2000180390A

    专利类型

  • 公开/公告日2000-06-30

    原文格式PDF

  • 申请/专利权人 JEOL LTD;

    申请/专利号JP19980354096

  • 发明设计人 YOSHIDA KOJI;

    申请日1998-12-14

  • 分类号G01N23/22;G01N23/225;

  • 国家 JP

  • 入库时间 2022-08-22 01:59:42

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