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BENZENECARBOXAMIDE COMPOUND AND GELLING AGENT OR SOLIDIFYING AGENT FOR ORGANIC LIQUID

机译:苯甲酰胺化合物和胶凝剂或有机液体固化剂

摘要

PROBLEM TO BE SOLVED: To obtain a new compound useful as a gelling agent or a solidifying agent in industrial fields including processing fields for coating materials, inks, lubricating oils, agricultures, fisheries, cosmetics or medicines, fibers, polymers, rubbers, metals, etc. ;SOLUTION: This compound is represented by formula I [X1 and X2 are each AA-NHR (AA is an amino acid acyl); R is an 8-22C alkyl; (n) is 1 or 2], e.g. N,N'-phthaloyl-bis(L-valylaminododecane). The compound represented by formula I can be produced by a method for reacting, e.g. an amino acid represented by the formula H-AA-OH with an alkylamine represented by the formula RNH2 at 0-100°C for 15-30 h, then reacting the resultant amino acid alkylamide represented by the formula H-AA-NHR with a benzenecarboxylic acid chloride represented by formula II in the presence of a base in a dry solvent at 0-100°C for 5-15 h and affording a benzenecarboxamide compound represented by formula III, etc.;COPYRIGHT: (C)2000,JPO
机译:要解决的问题:要获得在工业领域中用作胶凝剂或固化剂的新型化合物,包括涂料,油墨,润滑油,农业,渔业,化妆品或药品,纤维,聚合物,橡胶,金属,解决方案:该化合物由式I表示[X1和X2分别为AA-NHR(AA为氨基酸酰基);等等。 R为8-22C烷基; (n)为1或2],例如N,N′-邻苯二甲酰基双(L-戊酰氨基十二烷)。式I表示的化合物可以通过例如反应的方法制备。将式H-AA-OH表示的氨基酸与式RNH2表示的烷基胺在0-100℃下反应15-30小时,然后使式H-AA-NHR表示的氨基酸烷基酰胺与在干溶剂中于碱存在下,于0-100°C在碱的存在下,将式II表示的苯羧酸氯化物干燥5-15小时,得到式III表示的苯甲酰胺化合物等;版权所有:(C)2000,JPO

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