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METHOD FOR CHEMICAL VAPOUR INFILTRATION OF REFRACTORY SUBSTANCES, ESPECIALLY CARBON AND SILICON CARBIDE

机译:难溶物质,特别是碳和碳化硅的化学气相渗透方法

摘要

Disclosed is a method for chemical vapour infiltration (CVI) of refractory substances, especially an isothermic, isobaric method of CVI, especially of carbon (C) and silicon carbide (SiC), based on diffusion in a porous structure, whereby the pressure of the gas or partial pressure of an educt gas contained in the gas and the dwell time of the gas in the reaction zone are set at a given temperature in the reaction zone so that a separation reaction occurs in the porous structure in the area of pressure or partial pressure of the saturation adsorption of the gaseous and volatile compounds forming the solid phase. Saturation adsorption means that the separation speed remains substantially constant at an increased pressure of the gas or the partial pressure of the educt gas and the reaction of the educt gas is limited in such a way that no more than 50 % of the elements supplied in the educt gas forming the solid phase as it flows through the reaction zone are separated as a solid phase in the porous structure. The flow through the porous structure occurs in a straight line from bottom to top via slits substantially similar in width, ranging from 1-50 mm.
机译:本发明公开了一种基于难熔物质的化学气相渗透(CVI)的方法,特别是基于在多孔结构中的扩散的CVI的等温等压方法,尤其是碳(C)和碳化硅(SiC)的等温,等压方法。将气体中所含的离析气体的气体或分压以及反应区域中气体的停留时间设定为反应区域中的给定温度,从而在压力或分压区域内的多孔结构中发生分离反应。形成固相的气态和挥发性化合物饱和吸附的最大压力。饱和吸附是指在气体压力升高或离析气体分压时,分离速度基本保持恒定,并且离析气体的反应受到限制,以使进料中所含元素不超过50%。当固相流过反应区时形成固相的离析物气体在固相结构中被分离为多孔结构。通过多孔结构的流从底部到顶部通过一条宽度大致相同的狭缝以直线形式出现,范围为1-50 mm。

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