首页> 外国专利> Method of converting heavy fractions oil comprising a step of the distillation, the steps in an ebullating bed hydroconversion of the distillate under vacuum and residue under vacuum and a step of catalytic cracking.

Method of converting heavy fractions oil comprising a step of the distillation, the steps in an ebullating bed hydroconversion of the distillate under vacuum and residue under vacuum and a step of catalytic cracking.

机译:转化重馏分油的方法包括蒸馏步骤,在真空下对馏出物进行沸腾床加氢转化以及在真空下将残渣进行加氢转化的步骤以及催化裂化的步骤。

摘要

The hydrocarbons are distilled under vacuum, giving a distillate (DSV) and a residue (RSV). Part of the residue is hydrotreated and part is hydroconverted, producing liquids with reduced sulfur and metal content. These are distilled at atmospheric pressure, each giving a residue and a distillate. Part of the residue is treated in the presence of hydrogen in a treatment zone with a 3 phase reactor containing a boiling bed of hydrotreatment catalyst, in conditions which produce a liquid with reduced Conradson Carbon content, metals and sulfur. Part of the residue is treated in the presence of hydrogen in a hydroconversion section containing at least one 3-phase reactor containing at least one boiling bed of hydroconversion catalyst in conditions which produce a liquid with reduced Conradson Carbon content, in metals and sulfur. The hydrotreatment and hydroconversion reactors have upward gas and liquid flow with a catalyst extractor near the base of the reactor and a source of fresh catalyst near the top. The atmospheric distillations occur with an initial boiling point of about 300 deg C, more commonly between 350 and 370 deg C. The two atmospheric residues are mixed and sent to a catalytic cracker to obtain a gaseous fraction, a fuel fraction containing petrol and diesel, and a slurry. Part of the distillate under vacuum is mixed with the residue under vacuum during hydroconversion. The hydrotreatment and hydroconversion are at a pressure of between 2 and 35 MPa absolute and between 300 and 550 deg C, with a spatial duration of 0.1 to 10 per hour. The atmospheric distillations and distillation under vacuum have independent cutoff points of between 300 and 400 deg C, or the atmospheric distillations have the same cutoff between 300 and 400 deg C. Part of the atmospheric residue is returned to the hydroconversion and/or part to the refinery heavy fuel pool.
机译:在真空下蒸馏烃,得到馏出物(DSV)和残余物(RSV)。部分残余物经过加氢处理,部分经过加氢转化,生成的硫和金属含量降低了。将它们在大气压下蒸馏,各自给出残余物和馏出物。在含有氢处理催化剂沸腾床的三相反应器中,在存在氢气的条件下,在处理区中处理部分残余物,条件是产生的液体中康拉逊碳含量,金属和硫含量降低。在包含至少一个三相反应器的加氢转化段中,在氢存在下处理部分残余物,该三相反应器包含至少一个加氢转化催化剂的沸腾床,条件是产生的金属和硫的康拉逊碳含量降低。加氢处理和加氢转化反应器的气体和液体向上流动,在反应器底部附近有催化剂萃取器,在顶部附近有新鲜催化剂源。常压蒸馏的初始沸点约为300摄氏度,更常见的是在350至370摄氏度之间。将两种常压渣油混合并送入催化裂化器,以获得气态馏分,即包含汽油和柴油的燃料馏分,和泥浆在加氢转化期间,将真空下的一部分馏出物与真空下的残余物混合。加氢处理和加氢转化的压力为2至35 MPa绝对压力和300至550℃之间,空间持续时间为每小时0.1至10。常压蒸馏和真空蒸馏的截留点在300至400摄氏度之间,或者常压蒸馏具有相同的截留点在300至400摄氏度之间。部分常压渣油返回加氢转化和/或部分返回炼油厂重油库。

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