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Porous interfacial coating for fiber reinforced ceramic matrix composites

机译:纤维增强陶瓷基复合材料的多孔界面涂层

摘要

The present invention is embodied in ceramic matrix composites with porous interfacial coatings and the methods and processes for fabricating such coatings integral with the ceramic matrix composites. Each ceramic matrix composite of the present invention includes a fibrous substrate or fabric material with a porous interfacial coating. The coating, prior to processing, is comprised of a coating solution made of a carbon precursor and a ceramic precursor resin dissolved directly within a solvent or solvents. Fabrication is achieved by first desizing the fibrous substrate, second immersing the desized fibrous substrate in the mixed coating solution, third evaporating the solvent and curing the precursor and resin via a low temperature cure, and fourth pyrolyzing the coating via a high temperature pyrolysis, preferably in an inert atmosphere. Next, the coated fibrous substrate is combined with a ceramic matrix composite (CMC) . Last the coated fibrous substrate/CMC system is oxidized to remove the carbon particulates within the coating via high temperature air exposure to produce a CMC material with a porous interfacial coating.
机译:本发明体现在具有多孔界面涂层的陶瓷基复合材料中,以及与陶瓷基复合材料一体形成这种涂层的方法和工艺。本发明的每种陶瓷基复合材料包括具有多孔界面涂层的纤维基质或织物材料。在处理之前,涂层包括由碳前体和直接溶于一种或多种溶剂中的陶瓷前体树脂制成的涂层溶液。通过首先使纤维基材退浆,第二次将尺寸减小的纤维基材浸入混合的涂料溶液中,第三次蒸发溶剂并通过低温固化来固化前体和树脂,以及第四次通过高温热解将涂层热解来实现制造。在惰性气氛中。接下来,将涂覆的纤维基材与陶瓷基复合材料(CMC)结合。最后,经涂覆的纤维基材/ CMC系统被氧化以经由暴露于高温空气中以除去涂层内的碳颗粒,以产生具有多孔界面涂层的CMC材料。

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