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PROCESS FOR RECOVERY AND PURIFICATION OF SAPONINS AND SAPOGENINS FROM QUINOA (CHENOPODIUM QUINOA)

机译:奎奴亚藜中藜芦皂苷和皂苷元的回收和纯化工艺

摘要

The invention relates to a process for commercial extraction of saponins from quinoa, and optionally for the formation of corresponding sapogenins. The saponin extraction process comprises contacting a saponin-containing part of a quinoa plant (e.g. quinoa bran or seeds) with an aqueous alcohol solution containing an alcohol selected from methanol and ethanol to form a saponin-containing solution and an extracted solid residue, removing the alcohol from the saponin-containing solution to leave a saponin-containing aqueous solution, and evaporating water from the saponin-containing aqueous solution to produce a saponin-containing product. The conversion to sapogenins involves obtaining a solution of saponins in an aqueous alcohol, adding a strong acid to the solution to hydrolyze the saponins to form corresponding sapogenins that precipitate out of the solution as a precipitate, recovering the precipitate, and decolorizing the precipitate by forming a slurry of the precipitate with a solution of an aqueous base to form a decolorized sapogenin product. The processes of the invention permit efficient saponin extraction, and sapogenin production, on a commercial scale using inexpensive materials and techniques.
机译:本发明涉及从藜麦中商业提取皂苷,并任选地形成相应的皂苷元的方法。皂苷提取过程包括使藜麦植物的含皂苷的部分(例如藜麦或种子)与含有选自甲醇和乙醇的醇的醇水溶液接触,以形成含皂苷的溶液和提取的固体残留物,除去从含皂苷的溶液中除去乙醇以留下含皂苷的水溶液,并从含皂苷的水溶液中蒸发水以制备含皂苷的产物。转化为皂苷元的过程包括:获得皂苷在含水醇中的溶液,向该溶液中加入强酸以水解皂苷,形成相应的皂苷元,其从溶液中以沉淀形式沉淀出来,回收沉淀,并通过形成沉淀使沉淀脱色将沉淀物与碱水溶液混合,形成脱色的皂苷元产物。本发明的方法允许使用廉价的材料和技术以商业规模有效地提取皂苷和皂甙元。

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