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METHOD OF REUSING LEWISITE-TYPE SKIN ABSCESS-EFFECT POISON GASES
METHOD OF REUSING LEWISITE-TYPE SKIN ABSCESS-EFFECT POISON GASES
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机译:重用白榴石型皮肤止痛毒气的方法
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FIELD: poison disposal. SUBSTANCE: method involves alkali hydrolysis of lewisite with sodium hydroxide solution and is characterized by that hydrolyzed reaction mixture is further oxidized by aqueous solution of hydrogen peroxide at 60-80 C to give sodium arsenate. Resulting solution is concentrated until arsenate ion level arrives at 129 g/kg, cooled to 0-5 C, and sodium arsenate-dodecahydrate is then separated by filtration at pH 13. EFFECT: increased yield of sodium arsenate to 99%. 2 cl, 2 dwg
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机译:领域:毒物处置。物质:该方法涉及用氢氧化钠溶液对路易斯酸进行碱水解,其特征在于,水解的反应混合物在60-80℃下被过氧化氢水溶液进一步氧化,得到砷酸钠。将所得溶液浓缩直至砷酸根离子水平达到129 g / kg,冷却至0-5 C,然后在pH 13下过滤分离砷酸钠-十二水合物。效果:砷酸钠收率提高至99%。 2 cl,2 dwg
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