首页> 外国专利> DIAMOND-LIKE CRYSTALLINE BORON CARBIDE POWDER PRODUCT PRODUCTION PROCESS, THE PRODUCT MADE THEREBY AND ARRANGEMENT OF PILOT PLANT FOR THE PRODUCTION OF SAME

DIAMOND-LIKE CRYSTALLINE BORON CARBIDE POWDER PRODUCT PRODUCTION PROCESS, THE PRODUCT MADE THEREBY AND ARRANGEMENT OF PILOT PLANT FOR THE PRODUCTION OF SAME

机译:类金刚石晶体碳化硼粉的生产过程,由此生产的产品和用于生产相同产品的中试装置的布置

摘要

A process for manufacturing ultra fine pure diamond - like crystalline boron carbide powder from a composition of water soluble raw source materials, said processing of the composition comprising: choosing water soluble raw materials as soluble source chemicals charge composition for the processing of said composition for manufacturing ultra fine pure diamond - like crystalline boron carbide powder product; dissolving chosen soluble raw materials in the liquid medium for the subsequent processing; transporting said pure source charge solution to the drying stage of processing; drying the solution of the source chemicals charge composition, securing manufacturing of a voluminous dry charge powder, transporting said voluminous dry charge powder to the synthesis processing; synthesis processing, performed by means of thermal decomposition of said dry charge powder at elevated temperature in the presence of a controlled atmosphere and voluminous nucleating of the incipient multiple boron carbide crystals, wherein said choice of soluble chemical raw materials charge composition, used in the manufacturing process comprises: at least 1498 כ' בתמוז התשס" ב - June 30, 2002 one or more boron containing component(s), said boron containing components are chosen from a first group, but not limited to: boric acid, diboron trioxide, boron monoxide, boron and their mixtures; at least one or more carbon containing component(s), chosen from a second group, consisting, by way of example, but not limited to, of the saccharides dextrose, dextrose monohydrate, food sugar, fructose, glucose, glycogen, grape sugar, melassa, saccharose, sucrose and their mixtures; at least one or more activating chemical reagent(s), chosen from a third group, comprising, by way of example, but not limited to, the following organic acids and / or their mixtures: acetic acid, ascorbic acid, citric acid, decanoic acid, ethanoic acid, formic acid, fumaric acid, glacial acetic acid, glycolic acid, maleic acid, oxalic acid or oxalic acid dihydrate, peracetic acid, succinic acid; and optionally one or more chemical synergism component(s), comprising: acetic aldehyde, formic aldehyde, oxalic acid aldehyde and / or their derivatives; said dissolution medium is chosen from the group of: water, water + alcohol(s), and water + alcohol(s) + solvent(s), said chemical componenets composition being of the formulae: (a) boron carbide charge = Clx * C2y * C3w; and (b) boron carbide charge = Clx * C2y * C3w * C42; wherein: Cl is chemical raw material, chosen as above from the first group, with quantity factor " x" , expressed in gram molecular weight; C2 chemical raw material, chosen as above from the second gorup, with quantity factor " y" , expressed in gram molecular weight; C3 is chemical raw material, chosen as above from the third group, with quantity factor " w" , expressed in gram molecular weight; C4 is chemical raw material, chosen as above from the fourth group, with quantity factor " z" , expressed in gram mol weight, and said solution of raw chemical source materials composition does not emit any harmful vapors into the environment, thus rendering said process environmetally safe.
机译:一种由水溶性原料组合物制造超细纯金刚石状结晶碳化硼粉末的方法,所述组合物的处理包括:选择水溶性原料作为可溶性源化学品装料组合物,用于加工所述制造用组合物超细纯净的钻石-类结晶碳化硼粉末产品;将选定的可溶性原料溶解在液体介质中,以进行后续处理;将所述纯原料电荷溶液运输至处理的干燥阶段;干燥原料药装料组合物的溶液,确保制造大量的干装粉,将所述大量的干装粉运输到合成处理中;合成处理,是通过在受控气氛下在高温下将所述干装料粉末热分解并初生多个碳化硼晶体大量成核而进行的,其中所述可溶性化学原料装料组成的选择用于制造该方法包括:至少1498年-2002年6月30日,一种或多种含硼组分,所述含硼组分选自第一组,但不限于:硼酸,三氧化二硼,硼一氧化碳,硼及其混合物;至少一种或多种选自第二组的含碳组分,其例如但不限于由葡萄糖,一水葡萄糖,食物糖,果糖,葡萄糖,糖原,葡萄糖,蜜饯,蔗糖,蔗糖及其混合物;选自第三组的至少一种或多种活化化学试剂,其包括例如包括但不限于以下有机酸和/或它们的混合物:乙酸,抗坏血酸,柠檬酸,癸酸,乙酸,甲酸,富马酸,冰醋酸,乙醇酸,马来酸,草酸或草酸二水合物,过氧乙酸,琥珀酸;或任选地一种或多种化学协同组分,包括:乙醛,甲酸醛,草酸醛和/或其衍生物;所述溶解介质选自:水,水+醇和水+醇+溶剂,所述化学组分的组成式为:(a)碳化硼装料= Clx * C2y * C3w; (b)碳化硼装料= Clx * C2y * C3w * C42;其中:Cl是选自第一组的化学原料,具有以克分子量表示的数量因子“ x”; C2化学原料,是从第二种胶料中如上所述选择的,其数量因子“ y”以克分子量表示; C3是选自第三组的化学原料,其数量因子“ w”以克分子量表示; C4是选自第四组的化学原料,具有以克摩尔重量表示的量因子“ z”,并且所述化学原料原料组合物的溶液不向环境释放任何有害蒸气,因此使得所述方法对环境安全。

著录项

  • 公开/公告号IL126637B

    专利类型

  • 公开/公告日2002-06-30

    原文格式PDF

  • 申请/专利权人 ALEXANDER V ZARUEV;

    申请/专利号IL126637

  • 发明设计人

    申请日1998-10-18

  • 分类号6C04BA;

  • 国家 IL

  • 入库时间 2022-08-22 00:45:03

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