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Process for the preparation of lauryllactam by photonitrosation of cyclododecane and Beckmann rearrangement in the presence of methanesulphonic acid

机译:在甲烷磺酸存在下通过环十二烷的光亚硝化和贝克曼重排制备月桂内酰胺的方法

摘要

To the present invention:; a - it was also a cycloalkyl dissolved in an organic solvent, the reaction decane, nitrating agent and hydrogen chloride in the presence of an acid to form an oxime-cyclo dodecyl canon,; b - Only Beckman of the above oxime in the presence of an acid gaze will grow Nirvana; In the process for producing a la-lactam us configured, the acid relates to a method of producing la lauryl lactam, characterized in that methanesulfonic acid.
机译:对于本发明: a-也是在酸存在下溶于有机溶剂,癸烷,硝化剂和氯化氢的有机溶剂中形成的环烷基,形成肟-环十二烷基佳能; b-只有上述肟的贝克曼在酸性凝视的情况下才会生长必杀技;在所构造的la-内酰胺的制备方法中,所述酸涉及月桂基内酰胺的制备方法,其特征在于甲磺酸。

著录项

  • 公开/公告号KR100314982B1

    专利类型

  • 公开/公告日2001-11-30

    原文格式PDF

  • 申请/专利权人 아토피나;

    申请/专利号KR19990039567

  • 发明设计人 올리비에쟝;드뤼뗄다미앙;

    申请日1999-09-15

  • 分类号C07D227/02;

  • 国家 KR

  • 入库时间 2022-08-22 00:31:48

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