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- A method of determination of bisphenol-A in food and food packaging

机译:-食品和食品包装中双酚A的测定方法

摘要

PURPOSE: Provided is a detection method of bisphenol-A among foods or foods packing material which shows selective and superior sensitivity for gas chromatography(GC) or GC/mass spectrometer so that it provides optimal analysis condition for the GC/mass spectrometer. CONSTITUTION: The detection method of bisphenol-A among the foods or the foods packing material comprises the steps of: (i) extracting bisphenol-A from the foods or the foods packing material in organic solvent and treating in sodium hydroxide; (ii) reacting with 100-1400l of anhydrous acetic acid at 25-100deg.C for 5-20 minutes to produce derivatives of bisphenol-A; and (iii) analyzing concentration of bisphenol-A at the GC or the GC/mass spectrometer.
机译:目的:提供一种检测食品或食品包装材料中双酚A的方法,该方法对气相色谱(GC)或GC /质谱仪具有选择性和优越的灵敏度,从而为GC /质谱仪提供了最佳的分析条件。组成:在食品或食品包装材料中双酚A的检测方法包括以下步骤:(i)在有机溶剂中从食品或食品包装材料中提取双酚A并在氢氧化钠中处理; (ii)在25-100℃下与100-1400l无水乙酸反应5-20分钟,以产生双酚A的衍生物; (iii)在GC或GC /质谱仪上分析双酚A的浓度。

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