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Particle composition, useful as a disintergrating agent in compact, particulate wash- and cleaning agents, contains cross-linked polyvinylprrolidone having a specified particle size distribution

机译:用作致密,颗粒状洗涤和清洁剂中的崩解剂的颗粒组合物,包含具有规定粒径分布的交联聚乙烯基吡咯烷酮

摘要

A particle composition (I) contains particles of cross-linked polyvinylprrolidone having a particle size distribution in which as greater than 10 wt.% of particles have a particle size of less than 63 mu m, 0.1-30 wt.% of particles have a particle size greater than 1000 mu m and at least 10 wt.% of particles have a particle size of less than 200 mu m. Independent claims are included for: (i) a compact particulate wash and cleaning agent (II) containing 0.5-20 wt.% of the particle composition (I); (ii) a process for the production of the cleaning agent (II) by mixing 0.5-20 wt.% of the particle composition (I) with the other powdered ingredients; (iii) a process for the production of the particle composition (I) by means of popcorn polymerization by polymerization of a reaction mixture comprising N-vinylpyrrolidone and cross-linking agent in the absence of oxygen and polymerization initiators at upto 200 deg C in substance or using water as a precipitation agent and the particle size the popcorn polymer is controlled by introduction of an inert gas stream into the reaction mixture.
机译:颗粒组合物(I)包含具有粒径分布的交联聚乙烯基吡咯烷酮颗粒,其中大于10wt。%的颗粒具有小于63μm的粒径,0.1-30wt。%的颗粒具有小于100μm的粒径。大于1000μm的颗粒尺寸和至少10重量%的颗粒具有小于200μm的颗粒尺寸。包括以下独立权利要求:(i)包含0.5-20重量%的颗粒组合物(I)的紧凑的颗粒洗涤和清洁剂(II); (ii)通过将0.5-20重量%的颗粒组合物(I)与其他粉状成分混合来制备清洁剂(II)的方法; (iii)通过爆米花聚合反应制备颗粒组合物(I)的方法,该方法通过在不存在氧气的条件下使包含N-乙烯基吡咯烷酮和交联剂的反应混合物在不超过200℃的条件下聚合而进行。或使用水作为沉淀剂,并通过将惰性气体流引入反应混合物中来控制爆米花聚合物的粒径。

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