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Vaporizer tube for vaporizing liquid samples in capillary gas chromatography

机译:蒸发器管,用于在毛细管气相色谱法中蒸发液体样品

摘要

The invention relates to a vaporizer tube for vaporizing liquid samples in capillary gas chromatography. The vaporizer tube is open throughout its whole length. It has throats which are shaped to provide, in their region, a heavy increase of the flow velocity of the carrier gas, which flows substantially unrestrictedly through the vaporizer tube. This increase of the flow velocity causes, in accordance with Bernoulli's law, reduction in pressure. Due to this pressure reduction, the easily volatile solvent is predominantly volatilized. This vaporized solvent is carried along by the carrier gas flow. The solvent can then be removed through an outlet of the sample inlet chamber. The sample proper is vaporized in the larger diameter, low velocity zones between the throats by heating the vaporizer tube and are fed to the capillary column, after the solvent has been volatilized. Thus the vaporizer tube with a plurality of throats acts like a multi-plate column.
机译:本发明涉及一种用于在毛细管气相色谱法中蒸发液体样品的蒸发器管。蒸发器管在其整个长度上都是敞开的。它具有被设计成在其区域内大大增加载气流速的喉部,该载气基本上不受限制地流过蒸发器管。根据伯努利定律,流速的这种增加导致压力降低。由于该压力降低,易挥发的溶剂主要挥发。该汽化溶剂被载气流携带。然后可以通过样品入口室的出口除去溶剂。适当的样品通过加热蒸发器管在喉部之间的较大直径,低速区域中蒸发,并在溶剂挥发后送入毛细管柱。因此,具有多个喉部的蒸发器管的作用类似于多板塔。

著录项

  • 公开/公告号US2003017610A1

    专利类型

  • 公开/公告日2003-01-23

    原文格式PDF

  • 申请/专利权人 GERSTEL JOACHIM;

    申请/专利号US20020197633

  • 发明设计人 JOACHIM GERSTEL;

    申请日2002-07-16

  • 分类号G01N30/02;

  • 国家 US

  • 入库时间 2022-08-22 00:08:46

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