Dropping mercury electrode with mercury purification and recycling by means of contact with oxygenated water

摘要

An electroanalytical apparatus defining a Static Mercury Drop Electrode cell which includes a capillary tube at the end of which is formed mercury drops to constitute the working electrode including a container for continuously receiving and collecting mercury that has formed said working electrode and has become contaminated, a purifying vessel positioned in fixed relationship to the capillary tube, conduit means for continuously transferring mercury into the purifying vessel from the container, means for introducing highly oxygenated water into the purifying vessel at a location above the mercury collected in the vessel such that surface contact is established between said highly oxygenated water and the mercury collected in the purifying vessel, and means for continuously drawing mercury from the purifying vessel and feeding it as purified mercury to the capillary tube.