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A method for analysing metals in the fundamental state utilizing the statistical distribution of elements

机译:利用元素的统计分布分析基本态金属的方法

摘要

The present invention relates to a new analysis method to determine chemical compositions and states of metal materials. It includes the continuous steps of: using metallic discharge electrodes to perform the continuous spark discharge on the sample which is moved relative to the electrodes; dispersing the excited spark spectrum to form the linear spectrum with preset wavelength; recording the positions of every single spark discharge and the spectrum signals rapidly and at real-time; transferring the spectrum signals into electrical signals which are then inputted into signal memory; using a computer to statistically analyze the linear spectrum obtained from the single spark discharge, by which the distribution of chemical compositions, segregation, porosity and inclusion in the sample are resulted and then outputting these results. According to the present invention, the sample is subject to continuous excitation and synchronous scanning without pre-sparking, and every single spark spectrum signals is rapid collected and digital analyzed. Thus the original state of inclusion in sample without re-melting is obtained and various parameters for elements in sample, such as chemical compositions, segregation, porosity and inclusion content and distribution of these parameters are able to be simultaneously determined with one time scanning.
机译:本发明涉及确定金属材料的化学组成和状态的新分析方法。它包括以下连续步骤:使用金属放电电极对相对于电极移动的样品进行连续火花放电;分散激发的火花光谱,形成预设波长的线性光谱;快速,实时地记录每个火花放电的位置和频谱信号;将频谱信号转换成电信号,然后输入到信号存储器中;使用计算机对单次火花放电获得的线性光谱进行统计分析,由此得出样品中化学成分,偏析,孔隙率和夹杂物的分布,然后输出这些结果。根据本发明,对样品进行连续激发和同步扫描而没有预火花,并且快速采集每个火花光谱信号并进行数字分析。因此,无需重新熔融即可获得样品中夹杂物的原始状态,并且可以通过一次扫描同时确定样品中元素的各种参数,例如化学成分,偏析,孔隙率和夹杂物含量以及这些参数的分布。

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