首页> 外国专利> A process for the preparation of low-viscosity cellulose ethers by acidic - oxidative degradation of ground and dried cellulose ethers.

A process for the preparation of low-viscosity cellulose ethers by acidic - oxidative degradation of ground and dried cellulose ethers.

机译:一种通过研磨和干燥的纤维素醚的酸-氧化降解来制备低粘度纤维素醚的方法。

摘要

The invention relates to a method for the depolymerisation of cellulose ethers by means of acid oxidative decomposition. The ground and dried cellulose ether is first gassed with gaseous acid or is sprayed with the solution of an acid, and is brought into contact with an oxidant or a solution of an oxidant. It is then depolymerised at temperatures of between 50 and 120 DEG C for between 0.01 and 10 hours and the acid is neutralised by adding a base. The water content of the reaction mixture during the depolymerisation must not exceed 10 wt. %.
机译:本发明涉及一种通过酸氧化分解使纤维素醚解聚的方法。首先将磨碎并干燥的纤维素醚与气态酸一起充气,或将其喷入酸溶液,然后使其与氧化剂或氧化剂溶液接触。然后将其在50至120℃的温度下解聚0.01至10小时,并通过添加碱来中和酸。解聚过程中反应混合物的水含量不得超过10 wt。 %。

著录项

  • 公开/公告号DE10141680A1

    专利类型

  • 公开/公告日2003-03-13

    原文格式PDF

  • 申请/专利权人 CLARIANT GMBH;

    申请/专利号DE2001141680

  • 发明设计人 HAMMES ALF;

    申请日2001-08-25

  • 分类号C08B11/20;

  • 国家 DE

  • 入库时间 2022-08-21 23:42:41

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