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Method for the preparation of lactic acid and calcium sulphate and calcium sulphate dehydrate.

机译:制备乳酸和硫酸钙及脱水硫酸钙的方法。

摘要

Method for the preparation of lactic acid and calcium sulphate and calcium sulphate dehydrate.The invention relates to a method for the preparation of lactic acid and calcium sulphate.In which (a) an aqueous solution containing lactate is interacted with sulfuric acid at a temperature that is essentially larger than the transition temperature dehydrate calcium sulfate / semi- hydrated calcium sulphate (case ~ 4 ~.2H ~ 2 ~ / case ~ 4 ~ - 0,5h ~ 2 ~ the), to form a mixture which contains semi hydrated calcium sulfate and lactic acid.(b) the mixture of step (a) is subjected to at least one step of Recrystallization at a temperature that is lower than the transition temperature dehydrate calcium sulfate without /I - hydrated calcium sulphate dehydrate to form a precipitate of calcium sulfate and an aqueous solution of lactic acid.And (c) the precipitate of dehydrate calcium sulfate is separated from the aqueous solution of lactic acid.
机译:制备乳酸和硫酸钙以及脱水硫酸钙的方法。本发明涉及一种制备乳酸和硫酸钙的方法。(a)含乳酸的水溶液在一定温度下与硫酸相互作用。实质上大于过渡温度的脱水硫酸钙/半水合硫酸钙(案例〜4〜.2H〜2〜 /案例〜4〜-0.5h〜2〜的情况),形成包含半(b)使步骤(a)的混合物在低于转变温度的温度下进行至少一个重结晶步骤,使硫酸钙脱水而无水合硫酸钙脱水形成。 (c)将脱水硫酸钙的沉淀物从乳酸水溶液中分离出来。

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