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Perforated tray without downcomer, perforated tray tower without downcomer, and method of distillation

机译:无降液管的多孔塔板,无降液管的多孔塔板及其蒸馏方法

摘要

A perforated tray without downcomer in accordance with the present invention satisfies following conditions: (a) The hole has a diameter of 10mm to 25mm. (b) Two adjacent holes are spaced by a distance of 1.2d to 3d, measured between the two centers. (c) The tray thickness is 2mm to 8mm. (d) The opening ratio is 10% to 30%. A perforated tray tower without downcomer fitted with two or more such perforated trays without downcomer in accordance with the present invention satisfies following conditions: (g) Perforated trays are spaced by a distance of 0.1D to 0.5D (D denotes the tower diameter). (h) The levelness of each perforated tray is 8mm or less. (i) If a plurality of perforated trays are used at the same stage, the two most closely located holes that respectively belong to adjacent perforated trays are spaced by a distance of 50mm to 150mm, measured between the two centers. By using the perforated tray tower without downcomer, an easily polymerizable compound, such as an (meth)acrylic acid, or a liquid containing such an easily polymerizable compound can be distilled in a stable manner over an extended period of time with the formation of polymers being effectively prevented. IMAGE
机译:根据本发明的无降液管的多孔托盘满足以下条件:(a)孔的直径为10mm至25mm。 (b)两个相邻的孔在两个中心之间的距离为1.2d到3d。 (c)托盘厚度为2mm至8mm。 (d)开孔率为10%至30%。根据本发明的不具有降液管的多孔塔板装有两个或多个这样的不具有降液管的多孔塔板,其满足以下条件:(g)多孔塔板的间距为0.1D至0.5D(D表示塔的直径)。 (h)每个多孔托盘的水平度为8mm或更小。 (i)如果在同一阶段使用多个穿孔托盘,则分别属于相邻穿孔托盘的两个最靠近的孔之间的距离为两个中心之间的50mm至150mm。通过使用没有降液管的多孔塔板塔架,可以在形成聚合物的情况下长时间稳定地蒸馏出诸如(甲基)丙烯酸之类的易于聚合的化合物或含有这种易于聚合的化合物的液体。被有效预防。 <图像>

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