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A process of preparing for polysulfone-based hollow fiber membranes

机译:一种基于聚砜的中空纤维膜的制备方法

摘要

PURPOSE: A method for manufacturing polysulfone based hollow fiber membrane is provided to properly maintain separation and filtration performance of the hollow fiber membrane, prevent the hollow fiber membrane from being damaged and efficiently remove organic solvent remained in the hollow fiber membrane. CONSTITUTION: The method for manufacturing polysulfone based hollow fiber membrane comprises the processes of simultaneously discharging discharge dope and internal coagulant comprising polysulfone based resin, organic solvent and additive into air at a vertical lower side using a double tubular nozzle; sequentially passing the discharged discharge dope and internal coagulant through solidification tank in which outer coagulant is contained and cleaning tank in which cleaning solution is contained so that the discharge dope and internal coagulant are solidified and cleaned; and manufacturing the polysulfone based hollow fiber membrane by drying and winding the solidified and cleaned discharge dope and internal coagulant, wherein supersonic wave irradiating units are mounted on central part of the solidification tank and central part of the cleaning tank respectively to irradiate supersonic waves onto the discharge dope and internal coagulant, and wherein output of the supersonic wave irradiating units inside the solidification tank and the cleaning tank is 200 to 800 W, and irradiation distance thereof is 100 to 300 mm.
机译:目的:提供一种制造基于聚砜的中空纤维膜的方法,以适当地保持中空纤维膜的分离和过滤性能,防止中空纤维膜被损坏并有效地去除残留在中空纤维膜中的有机溶剂。构成:以聚砜为基的中空纤维膜的制造方法包括以下步骤:使用双管状喷嘴在垂直下侧将排放涂料和包含聚砜基树脂,有机溶剂和添加剂的内部凝结剂同时排入空气;使排出的浓液和内部混凝剂依次通过容纳有外部凝结剂的固化槽和容纳清洁液的清洁槽,以使排出的浓液和内部混凝剂固化和清洁。通过干燥和缠绕固化并清洁的排放涂料和内部凝结剂来制造聚砜类中空纤维膜,其中,在固化槽的中央部分和清洁槽的中央部分分别安装有超声波辐射单元,以将超声波辐射到聚砜基中空纤维膜上。排出涂料和内部凝结剂,其中,固化槽和清洗槽内的超声波照射单元的输出为200〜800W,照射距离为100〜300mm。

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