首页> 外国专利> Purifying 2,3-pyridine-dicarboxylic acid used as intermediate for e.g. drugs, by treatment in solution with sulfur source, removal of precipitate and precipitation with acid, giving low heavy metal content

Purifying 2,3-pyridine-dicarboxylic acid used as intermediate for e.g. drugs, by treatment in solution with sulfur source, removal of precipitate and precipitation with acid, giving low heavy metal content

机译:纯化用作例如中间体的2,3-吡啶-二羧酸。药物,通过在硫源溶液中处理,去除沉淀物并用酸沉淀,重金属含量低

摘要

Production of 2,3-pyridine-dicarboxylic acid (I) having a reduced heavy metal content comprises: (a) adding at least one sulfur source comprising hydrosulfides, sulfides, polysulfides or sulfur, to a solution of (I) or its salts; (b) removing the obtained precipitate from the solution; (c) acidifying the solution with mineral acid, and (d) recovering the precipitated (I).
机译:具有降低的重金属含量的2,3-吡啶-二羧酸(I)的生产包括:(a)将至少一种包含氢硫化物,硫化物,多硫化物或硫的硫源添加到(I)或其盐的溶液中; (b)从溶液中除去获得的沉淀; (c)用无机酸酸化溶液,和(d)回收沉淀的(I)。

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