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INTERNAL REFLUX TYPE MULTI-PURPOSE DISTILLATION TOWER, AND BATCH TYPE DISTILLATION METHOD USING THE SAME

机译:内回流式多用途蒸馏塔及使用该塔的间歇式蒸馏方法

摘要

PROBLEM TO BE SOLVED: To provide a multi-purpose distillation tower which is easy in changing the treatment of raw solution, and effective in separating highly value-added components of small amount by batch type or continuous type distillation.;SOLUTION: In the internal reflux type multi-purpose distillation tower, and batch type distillation method using the same, a distillation tower has a plurality of gas-liquid contact layers inside and a distillation vessel with a reboiler, a condenser unit for ascending vapor components is built in a tower top part, and a collector laminar layer in which descending condensate flows down in a displaceable manner in the direction of an inner circumferential wall of the tower is installed in a space part immediately below the condenser unit. A collector box of U-shaped section for the descending condensate is installed in the circumferential wall in the tower below the collector laminar layer. The collector box is divided into inner and outer chambers with bottom parts thereof communicating with each other by a partition plate installed in a concentric manner. A descending pipe for the in-tower reflux solution is provided in one divided chamber, and a distillate solution outwardly-discharging pipe is provided in the other divided chamber.;COPYRIGHT: (C)2005,JPO&NCIPI
机译:要解决的问题:提供一种多功能蒸馏塔,该蒸馏塔易于更改原料溶液的处理,并且可以通过分批式或连续式蒸馏有效地分离少量高附加值成分;解决方案:在内部回流式多用途蒸馏塔及使用该塔的间歇式蒸馏方法,在其内部具有多个气液接触层的蒸馏塔,具有再沸器的蒸馏容器,在塔内内置有用于使蒸气成分上升的冷凝器单元在冷凝器单元的正下方的空间部分设置有收集器层流层,在该收集器层流层中,下降的冷凝物沿塔的内周壁的方向以可移位的方式向下流动。用于下降的冷凝水的U形截面的收集箱安装在塔的收集壁层下方的圆周壁中。集电箱被分为内室和外室,其底部通过以同心方式安装的隔板彼此连通。塔内回流溶液的下降管设置在一个分隔室中,而馏出液向外排出管则设置在另一个分隔室中。版权所有:(C)2005,JPO&NCIPI

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