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The chromatograph column where the chromatograph column and before for the analysis preprocessing mannered

机译:色谱柱所在的色谱柱以及之前用于分析预处理的色谱柱

摘要

PROBLEM TO BE SOLVED: To provide a chromatograph column for refining a sample including a multicomponent organic compound such as each isomer of dioxins or the like simply and quickly, and being provided for analysis such as mass spectrometry or the like, and an analysis pretreatment method of an extraction liquid of the dioxins for refining the extraction liquid of the dioxins simply and quickly. SOLUTION: In this chromatograph column, a preceding column 1 and a subsequent column 2 are formed connectably and detachably, and sulfate silica gel is filled in the preceding column 1, and activated carbon silica gel and/or graphite carbon are filled in the subsequent column 2. In this analysis pretreatment method of the extraction liquid of the dioxins, the preceding column 1 and the subsequent column 2 are connected by using the chromatograph column, and after injecting the extraction liquid of the dioxins into the preceding column 1, a linear saturated hydrocarbon is injected into the preceding column 1 and discharged from the subsequent column 2, and then the preceding column 1 is detached from the subsequent column 2, and alkylbenzene is injected into the subsequent column 2.
机译:解决的问题:提供一种色谱柱,其用于简单且快速地精制包含多组分有机化合物(例如二恶英的各个异构体等)的样品,并提供用于质谱分析等分析以及分析预处理方法二恶英的提取液的制备,用于简单,快速地精制二恶英的提取液。解决方案:在该色谱柱中,前一列和后一列2可连接和可拆卸地形成,硫酸硅胶被填充到前一列中,而活性炭硅胶和/或石墨碳被填充在后一列中。 2.在该二恶英提取液的分析预处理方法中,前色谱柱1和后色谱柱2通过色谱柱连接,将二恶英提取液注入前色谱柱1后,呈线性饱和状态。将烃注入前一个塔1中并从后一个塔2中排出,然后将前一个塔1与后一个塔2分离,并将烷基苯注入后一个塔2中。

著录项

  • 公开/公告号JP3656527B2

    专利类型

  • 公开/公告日2005-06-08

    原文格式PDF

  • 申请/专利权人 JFEスチール株式会社;

    申请/专利号JP20000228493

  • 发明设计人 志村 眞;花田 一利;

    申请日2000-07-28

  • 分类号G01N30/46;B01D15/08;G01N30/26;G01N30/48;G01N30/88;G01N33/00;

  • 国家 JP

  • 入库时间 2022-08-21 22:27:03

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