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METHODS OF OBTAINING THE NANOCOMPOSITE FERROMAGNETIC POWDER

机译:获得纳米复合铁磁粉的方法

摘要

Invention relates to the field of powder metallurgy, in particular, to the methods of obtaining the nanodispersed powders of metals and alloys, and it can be used in chemical industry and materials science for production of nanostructural materials of technical purpose on their basis. Synthesis is proposed, consisting of interaction of salts of metals of iron, cobalt and nickel in the presence of alcohols and tartaric acid, starch precipitated by oxalic acid. The reduction of the powders of oxalates of metals is carried out at a temperature of 380-400 °?? in different reducing atmospheres. Proposed synthesis allows to obtain nanocomposite ferromagnetic powder, which is not pyrophoric, does not light up, is corrosion-resistant, with hydrophilic surface, withstands the heating temperature up to 100 °??, with the size of particles in nanodispersed range. Invention allows to obtain nanostructural ferromagnetic powders with assigned combination of properties achieved simultaneously.
机译:本发明涉及粉末冶金领域,尤其涉及一种金属和合金的纳米分散粉末的制备方法,可在化学工业和材料科学中用于以其为基础生产纳米结构材料。提出了合成方法,该方法包括在醇和酒石酸存在下,铁,钴和镍的金属盐之间的相互作用,以及草酸沉淀的淀粉。金属草酸盐粉末的还原是在380-400℃的温度下进行的。在不同的还原气氛中。拟议的合成方法可以得到纳米复合铁磁性粉末,该粉末不发火,不发光,耐腐蚀,具有亲水性表面,可承受高达100°C的加热温度,且粒径在纳米分散范围内。本发明允许获得具有同时实现的性能的指定组合的纳米结构铁磁粉末。

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