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A method for manufacturing extraction rosin for extraction and separation of an rare earth element

机译:一种用于提取和分离稀土元素的提取松香的方法

摘要

PURPOSE: Provided is a process for producing an extracting resin for extracting and separating a rare earth element, which can make a separating and refining process simple, regenerate semipermanently, and easily separate the rare earth element in high purity. CONSTITUTION: The process comprises the steps of: preparing a copolymer by injecting an initiator into a mixture of distilled water, styrene, and divinyl benzene; adding a rare earth element extracting agent, a dispersant, a stabilizer, a pore forming agent to the copolymer preparing step; stirring at 70-90deg.C and 400-2000rpm and then post-treating, wherein the post-treating comprises the steps of: reacting at 70-90deg.C for 12-24 hours and then cooling slowly and filtering the extracting resin; cleaning for 10-60 min. with an alcohol and drying. The initiator is selected from a benzoyl peroxide or azobis isobutyronitrile and the extracting agent is bisdiethyl hexyl phosphinic acid.
机译:目的:提供一种用于提取和分离稀土元素的提取树脂的方法,该方法可以使分离和精制过程变得简单,半永久性再生,并且容易以高纯度分离稀土元素。组成:该方法包括以下步骤:通过将引发剂注入蒸馏水,苯乙烯和二乙烯基苯的混合物中来制备共聚物;在共聚物制备步骤中加入稀土元素萃取剂,分散剂,稳定剂,成孔剂。在70-90℃和400-2000rpm下搅拌,然后进行后处理,其中后处理包括以下步骤:在70-90℃下反应12-24小时,然后缓慢冷却并过滤萃取树脂;清洁10-60分钟。用酒精干燥。引发剂选自过氧化苯甲酰或偶氮二异丁腈,萃取剂为双二乙基己基次膦酸。

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