METHOD voltammetric analysis of the phase and elemental composition of objects AND DEVICE FOR IMPLEMENTATION

摘要

1.method u0432u043eu043bu044cu0442u0430u043cu043fu0435u0440u043eu043cu0435u0442u0440u0438u0447u0435u0441u043au043eu0433u043e analysis phase and elemental composition of the object, including the background u044du043bu0435u043au0442u0440u043eu043bu0438u0442u0430 contact with substance in test object the proposal by the electric u043du0430u043fu0440u00a0u0436u0435u043du0438u00a0 to u043fu043eu043bu00a0u0440u0438u0437u0443u044eu0449u0435u043cu0443 and working electrodes and u0441u043du00a0u0442u0438u0435 u0432u043eu043bu044cu0442u0430u043cu043fu0435u0440u043du043eu0439 characteristics, u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 what've background olita u043fu0440u0438u043cu0435u043du00a0u044eu0442 solid electrolyte.electrochemically stable in the working area of the capacity.;2. method u0432u043eu043bu044cu0442u0430u043cu043fu0435u0440u043eu043cu0435u0442u0440u0438u0447u0435u0441u043au043eu0433u043e analysis 1, u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0, however, that the above solid electrolyte is used as a part of the working electrode.;3. method u0432u043eu043bu044cu0442u0430u043cu043fu0435u0440u043eu043cu0435u0442u0440u0438u0447u0435u0441u043au043eu0433u043e analysis 1, u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0, u0443u043fu043eu043cu00a0u043du0443u0442u044bu0439 contact background u044du043bu0435u043au0442u0440u043eu043bu0438u0442u0430 with substance test object u043eu0441u0443u0449u0435u0441u0442u0432u043bu00a0u044eu0442 time eat solid u044du043bu0435u043au0442u0440u043eu043bu0438u0442u0430 clipping thereof to the surface of the test object with an effective effort and u0432u0440u0435u043cu00a0, adequate means of sorption u0434u043bu00a0 u0433u0435u0442u0435u0440u043eu0444u0430u0437u043du043eu0439 anymore in the test object.;4. method u0432u043eu043bu044cu0442u0430u043cu043fu0435u0440u043eu043cu0435u0442u0440u0438u0447u0435u0441u043au043eu0433u043e analysis 1, u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0, u0443u043fu043eu043cu00a0u043du0443u0442u044bu0439 contact background u044du043bu0435u043au0442u0440u043eu043bu0438u0442u0430 with substance test object u043eu0441u0443u0449u0435u0441u0442u0432u043bu00a0u044eu0442 time eat the mechanical u0432u0432u0435u0434u0435u043du0438u00a0 sample substances in the above solid u044du043bu0435u043au0442u0440u043eu043bu0438u0442u0430 or u043du0430u043du0435u0441u0435u043du0438u00a0 sample substance on its surface.;5. method u0432u043eu043bu044cu0442u0430u043cu043fu0435u0440u043eu043cu0435u0442u0440u0438u0447u0435u0441u043au043eu0433u043e analysis on any of the u043fu043f.1 - 4, u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 so that as the above solid u044du043bu0435u043au0442u0440u043eu043bu0438u0442u0430 use u0438u043eu043du043eu043fu0440u043eu0432u043eu0434u00a0u0449u0438u0439 u043fu043eu043bu0438u043cu0435 r.;6. the device u0434u043bu00a0 u043eu0441u0443u0449u0435u0441u0442u0432u043bu0435u043du0438u00a0 method u0432u043eu043bu044cu0442u0430u043cu043fu0435u0440u043eu043cu0435u0442u0440u0438u0447u0435u0441u043au043eu0433u043e analysis on p.5, containing the working electrode, the electrode u0441u0440u0430u0432u043du0435u043du0438u00a0 and / or u043fu043eu043bu00a0u0440u0438u0437u0443u044eu0449u0438u0439 electrode electrically connected to the source of u043du0430u043fu0440u00a0u0436u0435u043du0438u00a0, u043eu0442u043bu0438u0447u0430u044eu0449u0435u0435u0441u00a0 what to u0440u043fu0443u0441 is designed in the form of u0441u0442u0435u0440u0436u043du00a0 u0434u0438u044du043bu0435u043au0442u0440u0438u0447u0435u0441u043au043eu0433u043e material, / which establishes u0443u043fu043eu043cu00a0u043du0443u0442u044bu0435 electrodes so that the free ends of the electrode u0441u0440u0430u0432u043du0435u043du0438u00a0 and / or u043fu043eu043bu00a0u0440 u0438u0437u0443u044eu0449u0435u0433u043e electrode electrically connected with the u0438u043eu043du043eu043fu0440u043eu0432u043eu0434u00a0u0449u0438u043c polymer.a free end of the electrode is able to contact with either u0438u043eu043du043eu043fu0440u043eu0432u043eu0434u00a0u0449u0438u043c polymer, either directly from the analyzed object.