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Method for separating para-xylene and a clay treatment step at least one located upstream of the adsorption zone and the crystallization step at least one high temperature

机译:分离对二甲苯的方法和至少一个位于吸附区上游的粘土处理步骤以及至少一个高温的结晶步骤

摘要

In the method for separating para-xylene of very high purity from [summary] xylene isomers feed, selective adsorption step of fraction rich in para-xylene (8), (57) the method, at least one of the high-temperature It includes crystallization step portion of Tsu and (5a), the isomerization process of the fraction is poor in p-xylene and (21), in some cases, if the clay treatment step followed (26), the mother liquor (3) The recycled to (8) Selective adsorption step via distillation step of the treated effluent (28) by. The mother liquor may be introduced into (23) in the distillation apparatus following the isomerization step before being treated clay in the reactor. The crystallization process includes several steps at high temperature, the temperature in one step of one of these stages is a low temperature or a higher temperature than in a separate step. It is applied to the production of paraxylene very pure for the synthesis of terephthalic acid.
机译:在从[二甲苯]异构体原料中分离非常高纯度的对二甲苯的方法中,对富含对二甲苯的馏分进行选择性吸附的步骤(8),(57)是至少一种高温的方法,包括Tsu和(5a)的结晶步骤部分,馏分的异构化过程在对二甲苯和(21)中较差,在某些情况下,如果接着(26)进行粘土处理步骤,则将母液(3)再循环至(8)选择性蒸馏步骤是通过蒸馏步骤处理的流出物(28)。在异构化步骤之后,可以将母液引入蒸馏设备中的(23)中,然后在反应器中对其进行处理。结晶过程包括高温下的几个步骤,这些步骤之一的一个步骤中的温度是低温或高于单独步骤中的温度。它用于生产对苯二酸非常纯的对二甲苯。

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