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Process for preparing perovskite-type crystalline compound powders

机译:钙钛矿型结晶化合物粉末的制备方法

摘要

A process for preparing perovskite-type compound Ax(BO3)y powders involving reacting a solution containing A and a solution containing B, or a combined solution comprising A and B, with an alkaline solution in a high-gravity reactor at a temperature ranging from about 60° C. to about 100° C. A is one or more metal elements selected from the group consisting of Li, Na, K, Mg, Ca, Sr, Ba, Pb, Sm, La, Nd, Bi, and other rare-earth metal elements. B is one or more metal elements selected from the group consisting of Ti, Zr, Sn, Hf, Nb, Ce, Al, Zn, Mn, Co, Ni, Fe, Cr, Y, Sc, W, Ta, and the like. The resulting mixture is then filtered, rinsed and dried to obtain the desired powders. The obtained perovskite-type compound Ax(BO3)y powders have a small average particle size with a narrow particle size distribution, a perfect crystal form and a uniform particle shape, and is suitable for use as raw material for making dielectric, piezoelectric, anti-ferroelectric, pyroelectric, pressure-resisting, sensing, microwave media, and other ceramics.
机译:制备钙钛矿型化合物A x (BO 3 y 粉末的方法,该方法包括使含有A的溶液和含有B的溶液反应,或在高重力反应器中,在约60°C至约100°C的温度范围内,将包含A和B的混合溶液与碱性溶液混合。A是一种或多种选自Li,Na ,K,Mg,Ca,Sr,Ba,Pb,Sm,La,Nd,Bi和其他稀土金属元素。 B是选自Ti,Zr,Sn,Hf,Nb,Ce,Al,Zn,Mn,Co,Ni,Fe,Cr,Y,Sc,W,Ta等的一种或多种金属元素。 。然后将所得混合物过滤,冲洗并干燥以获得所需粉末。所得钙钛矿型化合物A x (BO 3 )y粉末具有较小的平均粒径和窄的粒径分布,完美的晶体形式和均匀的颗粒形状,并且适合用作制造介电,压电,反铁电,热释电,耐压,传感,微波介质和其他陶瓷的原料。

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