首页> 外国专利> TWO-STAGE METHOD FOR THE PRODUCTION OF TRIOXANE FROM A HIGHLY CONCENTRATED AQUEOUS FORMALDEHYDE SOLUTION, THE REACTION MIXTURE BEING STRIPPED FROM THE SYNTHESIS REACTOR IN A GASEOUS FORM AND BEING TRANSFERRED INTO A DISTILLATION COLUMN

TWO-STAGE METHOD FOR THE PRODUCTION OF TRIOXANE FROM A HIGHLY CONCENTRATED AQUEOUS FORMALDEHYDE SOLUTION, THE REACTION MIXTURE BEING STRIPPED FROM THE SYNTHESIS REACTOR IN A GASEOUS FORM AND BEING TRANSFERRED INTO A DISTILLATION COLUMN

机译:从高浓度甲醛水溶液生产三恶烷的两步法,反应混合物以气态形式从合成反应器中分离出来,然后转移到蒸馏塔中

摘要

The invention relates to a method for producing raw trioxane, comprising the following stages: - a highly concentrated aqueous formaldehyde solution is subjected to an acid catalyzed reaction so as to obtain a trioxane/formaldehyde/water mixture (stage I); and - the trioxane/formaldehyde/water mixture obtained in stage I is distilled in order to obtain raw trioxane (stage II). The inventive method is characterized in that the trioxane/formaldehyde/water mixture is stripped from the synthesis reactor (R) in a gaseous form in stage I.
机译:本发明涉及一种生产粗三恶烷的方法,包括以下步骤:-使高浓度的甲醛水溶液经受酸催化反应,以获得三恶烷/甲醛/水混合物(步骤I); -蒸馏步骤I中得到的三恶烷/甲醛/水混合物以获得粗制三恶烷(步骤II)。本发明方法的特征在于,在阶段I中以气态形式从合成反应器(R)中汽提三恶烷/甲醛/水混合物。

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