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The nuclear magnetic resonance device which features

机译:核磁共振装置的特点

摘要

There is providesd a nuclear magnetic resonance spectrometer having a high sensitiveness by simultaneously realizing a high uniformity of a static magnetic field and a high measuring sensitiveness. A sample tube used in the nuclear magnetic resonance spectrometer is constructed in a structure in which the shape of a sample placed in a measuring space can be changed. The change in shape of the sample can be achieved by controlling the pressure applied to the sample. There is at least one surface of contact between the sample placed in the measuring space and a gas existing around the sample, and the shape of such surface is maintained by the surface tension of the sample. In this case, a central portion of a magnet, into which the sample tube is inserted, filled with a sterilizing gas having a pressure higher than the atmospheric pressure, and the sample having a surface of contact with the gas is maintained in a sterile state. A measuring coil used in the nuclear magnetic resonance spectrometer is disposed on a rotatable curved surface symmetrical with respect to a rotational axis provided by a longitudinal center axis of the sample tube.
机译:通过同时实现静磁场的高度均匀性和高测量灵敏度,提供了具有高灵敏度的核磁共振光谱仪。核磁共振波谱仪中使用的样品管构造成可以改变放置在测量空间中的样品的形状的结构。样品形状的改变可以通过控制施加到样品上的压力来实现。放置在测量空间中的样品与样品周围存在的气体之间至少有一个接触表面,并且该表面的形状由样品的表面张力保持。在这种情况下,插入有样品管的磁体的中央部分填充有压力高于大气压的灭菌气体,并且具有与气体接触的表面的样品保持无菌状态。 。核磁共振波谱仪中使用的测量线圈设置在相对于由样品管的纵向中心轴提供的旋转轴对称的可旋转曲面上。

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