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Process for producing micro-mesoporous metal oxide having regulated pores formed by novel template removal method

机译:通过新型模板去除方法制备具有调节孔的微孔金属氧化物的方法

摘要

The present invention is the method for preparation of transition metal oxide having micro-mesoporous structure whose average fine pores size is not less than 1 nm and not more than 2 nm comprising, adding and dissolving transition metal salt which is a precursor of transition metal oxide and/or metal alkoxide in the solution prepared by dissolving polymer surfactant in organic solvent, hydrolyzing said transition metal salt and/or metal alkoxide and preparing sol solution which is polymerized and self organized, then obtaining gel whose organization is stabilized from said sol solution and removing said polymer surfactant by using water of room temperature or water to which alkali metal or alkaline earth metal ion is added.
机译:本发明是具有平均细孔尺寸为1nm以上且2nm以下的微中孔结构的过渡金属氧化物的制备方法,其包括添加,溶解作为过渡金属氧化物的前体的过渡金属盐。通过将聚合物表面活性剂溶解在有机溶剂中,水解所述过渡金属盐和/或金属醇盐并制备聚合和自组织的溶胶溶液,然后从该溶胶溶液中获得其组织稳定的凝胶,来制备溶液中的金属和/或金属醇盐。通过使用室温的水或添加了碱金属或碱土金属离子的水除去所述聚合物表面活性剂。

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