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METHOD FOR THE PRODUCTION OF ANHYDROUS ANHYDROUS RAR-EARTH METAL HALDES, SYNTHESIS MIXTURES CONTAINING ANHYDROUS RARE-EARTH METAL HALIDES AND USE THEREOF
METHOD FOR THE PRODUCTION OF ANHYDROUS ANHYDROUS RAR-EARTH METAL HALDES, SYNTHESIS MIXTURES CONTAINING ANHYDROUS RARE-EARTH METAL HALIDES AND USE THEREOF
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机译:无水无水稀土金属卤化物的生产方法,包含无水稀土金属卤化物的合成混合物及其用途
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摘要
The invention relates to a method wherein rare earth metal oxides are reacted with halogenation agents of general formula (1), wherein M=Si, Ge, Sn, Ti, Zr, Hf; Hal=CI, Br, I; X1, X2, X3 = independently from each other CI, Br, I, H, alkoxy (-OR), wherein R represents an organo radical having 1-20 atoms, alkyl having 1-20 C atoms or aryl with 6-20 C atoms, wherein the alkyl or arly radicals can include one or several halogen substituents selected from the group of F, CI, Br or I; in an aprotic polar solvent. The invention also relates to synthesis mixtures containing water-free rare earth metal halogenides and the use thereof.
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机译:本发明涉及一种方法,其中稀土金属氧化物与通式(1)的卤化剂反应,其中M = Si,Ge,Sn,Ti,Zr,Hf;和Hal = CI,Br,I; X 1,X 2,X 3彼此独立地为Cl,Br,I,H,烷氧基(-OR),其中R表示具有1-20个原子的有机基团,具有1-20个碳原子的烷基或具有6-20个碳原子的芳基原子,其中烷基或芳基可包括一个或多个选自F,Cl,Br或I的卤素取代基;在非质子极性溶剂中。本发明还涉及含有无水稀土金属卤化物的合成混合物及其用途。
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