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Continuous process for obtaining and / or for the preparation of polysaccharide derivatives.

机译:获得和/或制备多糖衍生物的连续方法。

摘要

Procedure for obtaining and / or developing continuously polysaccharide derivatives by reaction and / or conditioning in a suspension with components of the liquid reaction, characterized in that, according to Figure 1 a) is introduced continuously a current in suspension, preheated if appropriate to 185 ° C, consisting of solids SE and liquid phase LE, in the head of a column which is, if appropriate, under a pressure cushion of up to 6 * 106 Pa, that is largely filled with a different liquid phase L, identical or heated to the same temperature, then b) the solids SE freely sedimented to the bottom of the column, under the action of gravity, through the liquid phase L, transforming the solid matter in the solids SA by reaction and / or conditioning with the liquid phase L and c) are removed from the gas column G, asc endentes optionally travésde the head of the column and d) is discharged solid matter SA, continuously, as a stream in suspension, the bottom of the column, again by adding liquid phase LR, previously withdrawn from the top of the column and conveyed to the bottom of the column through a separate and / or new liquid phase LN connection dosed from the outside on the bottom of the column, maintaining constant the filling level of the column.
机译:通过与液体反应组分在悬浮液中反应和/或调节来获得和/或连续开发多糖衍生物的方法,其特征在于,根据图1a),在悬浮液中连续引入电流,如果合适,将其预热至185° C,由固体SE和液相LE组成,位于塔的顶部,如果合适的话,在最高6 * 106 Pa的压力垫下,该塔中主要装有相同的或加热至在相同的温度下,然后b)固体SE在重力的作用下通过液相L自由地沉淀到塔底,通过与液相L的反应和/或调节使固体SA中的固体物质转化c)和c)从气塔G中移出,asc选择性地穿过塔的顶部,并且d)再次以悬浮液的形式连续地将固体物质SA排放到塔底,再通过添加预先从塔顶抽出的液相LR通过从塔底外部注入的单独的和/或新的液相LN连接输送到塔底,以保持塔顶液位恒定。柱。

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