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PREPARATION OF DI-t-ALKYL PEROXIDES AND t-ALKYL HYDROPEROXIDES FROM n-ALKYL t-ALKYL ETHERS
PREPARATION OF DI-t-ALKYL PEROXIDES AND t-ALKYL HYDROPEROXIDES FROM n-ALKYL t-ALKYL ETHERS
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机译:由正烷基叔烷基醚制备二叔烷基过氧化物和叔羟基过氧化物
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摘要
A process for production of a t-alkyl peroxide compound includes the steps of:a) reacting an n-alkyl t-alkyl ether with a reactant mixture comprising an acid catalyst and a compound of the formula where R is H or t-alkyl, provided that if R is t-alkyl the t-alkyl peroxide compound product is a di-t-alkyl peroxide,andb) isolating a reaction product comprising said t-alkyl peroxide compound from the mixture resulting from step a).The process can be used to prepare t-butyl hydroperoxide or di-t-butyl peroxide from methyl t-butyl ether. Sulfuric acid may be used as the acid catalyst.
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