首页> 外国专利> ORGANIC-INORGANIC HYBRID HARD COATING COMPOSITIONS AND THEIR PREPARATION METHOD WITH IMPROVED STABILITY FOR STORAGE AND WORKABILITY

ORGANIC-INORGANIC HYBRID HARD COATING COMPOSITIONS AND THEIR PREPARATION METHOD WITH IMPROVED STABILITY FOR STORAGE AND WORKABILITY

机译:有机-无机混合硬质涂料组合物及其制备和储存稳定性提高的制备方法

摘要

Provided are a method for preparing a transparent coating agent, a transparent coating agent composition, a method for preparing a colored coating agent, and a colored coating agent composition to improve working stability and storage stability by using colloidal silica sol and silane. The preparation method of a transparent coating agent comprises the steps of mixing a silica sol, a silane, an alcohol and a catalyst with stirring to prepare a solution A; mixing a silane and a catalyst with stirring to prepare a solution B; and mixing the solution A and the solution B with stirring and maturing the mixture at a room temperature for a certain time. The transparent coating agent composition comprises 10-60 parts by weight of colloidal silica; 10-50 parts by weight of a first silane; 10-40 parts by weight of an alcohol; and 0.5-5 parts by weight of an acid, wherein the first silane is represented by RSi(OR')3; R is CH3, CH2CH3, CH2CH2CH3, CH2CH2CH2CH3, C6H5 or CH2CH2CH2CH2CH2CH2CH2CH3; and the acid is hydrofluoric acid, hydrochloric acid, sulfuric acid, nitric acid, formic acid, propionic acid or acetic acid.
机译:本发明提供通过使用胶体二氧化硅溶胶和硅烷来提高加工稳定性和保存稳定性的透明涂布剂的制备方法,透明涂布剂组合物,着色涂布剂的制备方法以及着色涂布剂组合物。透明涂层剂的制备方法包括以下步骤:在搅拌下将硅溶胶,硅烷,醇和催化剂混合以制备溶液A。在搅拌下将硅烷和催化剂混合以制备溶液B;在搅拌下将溶液A和溶液B混合并在室温下熟化一定时间。透明涂层剂组合物包含10-60重量份的胶态二氧化硅;优选为10-60重量份。 10-50重量份的第一硅烷; 10-40重量份的酒精; 0.5-5重量份的酸,其中第一硅烷由RSi(OR′)3表示; R为CH 3,CH 2 CH 3,CH 2 CH 2 CH 3,CH 2 CH 2 CH 2 CH 3,C 6 H 5或CH 2 CH 2 CH 2 CH 2 CH 2 CH 2 CH 2 CH 3;所述酸为氢氟酸,盐酸,硫酸,硝酸,甲酸,丙酸或乙酸。

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