首页>
外国专利>
process for the production of 2,4,4,6 - tetrabrom - 2.5 - cyclohexadienon
process for the production of 2,4,4,6 - tetrabrom - 2.5 - cyclohexadienon
展开▼
机译:2,4,4,6-四溴-2.5-环己二酮的生产方法
展开▼
页面导航
摘要
著录项
相似文献
摘要
A highly pure 2,4,4,6-tetrabromo-2,5-cyclohexadienone has been prepared in a single pot, eco-friendly procedure in yields of 91-94 % from phenol. In this method, a mixture of alkali/alkaline earth metal bromide and alkali/alkaline earth metal bromate was employed as brominating agent in place of corrosive liquid bromine. The reaction between phenol and the brominating reagent was initiated by the action of a mineral acid or moderately strong organic acid. The crude product was further characterized by standard analytical and spectroscopic methods.
展开▼