首页> 外国专利> POLYVINYL ACETAL RESIN, METHOD AND APPARATUS FOR PRODUCING THE SAME, AND ADHESIVE AND CIRCUIT BOARD USING THE POLYVINYL ACETAL RESIN

POLYVINYL ACETAL RESIN, METHOD AND APPARATUS FOR PRODUCING THE SAME, AND ADHESIVE AND CIRCUIT BOARD USING THE POLYVINYL ACETAL RESIN

机译:聚乙烯醇缩醛树脂,其制备方法和装置以及使用该聚乙烯醇缩醛树脂的胶粘剂和电路板

摘要

PROBLEM TO BE SOLVED: To provide a polyvinyl acetal resin which is reduced in the content of chlorine.;SOLUTION: The polyvinyl acetal resin containing ≤8 ppm chlorine is provided. The polyvinyl acetal resin can be produced, for example, by a method which comprises (1) an acetalization reaction process: a process of reacting a polyvinyl alcohol to acetalize with an aldehyde in the presence of an acid catalyst at 20-50°C reaction temperature, with ≥0.3 kW/m3 agitation power per unit volume and in ≥10 minutes average retention time, (2) a primary washing process: a process of preparing a primary cake of a polyacetal resin by pre-dehydrating the reaction product of the acetalization reaction, adding ≤40°C water to bring the product to be a slurry, washing and dehydrating the same and (3) a reslurry washing process: a process of adding ≤40°C water to the primary cake to reslurry the same, washing, dehydrating and drying the same.;COPYRIGHT: (C)2008,JPO&INPIT
机译:解决的问题:提供一种减少氯含量的聚乙烯醇缩醛树脂。解决方案:提供含氯含量小于等于8 ppm的聚乙烯醇缩醛树脂。聚乙烯醇缩醛树脂可以例如通过以下方法来制造:(1)缩醛化反应工序:在酸催化剂的存在下,在20〜50℃下使聚乙烯醇与醛缩醛化的工序。温度,每单位体积的搅拌功率为≥ 0.3 kW / m 3 ,平均保留时间为10分钟以内,(2)初次洗涤过程:制备聚缩醛初筛的过程通过将缩醛化反应的反应产物预脱水,加入40℃的水使产物成为淤浆,对其进行洗涤和脱水,以及(3)再淤浆洗涤过程:加入-40%的过程; C水至原饼相同的浆液,洗涤,脱水,干燥相同。;版权所有:(C)2008,日本特许厅

著录项

  • 公开/公告号JP2008222938A

    专利类型

  • 公开/公告日2008-09-25

    原文格式PDF

  • 申请/专利权人 DENKI KAGAKU KOGYO KK;

    申请/专利号JP20070066018

  • 申请日2007-03-15

  • 分类号C08F16/38;C08F8/28;C08F6/00;C08F2/01;C09J129/14;H05K1/03;

  • 国家 JP

  • 入库时间 2022-08-21 20:25:26

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