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Method and apparatus for separating volatile compounds during the polycondensation reaction and to generate a pressure reduction

机译:在缩聚反应过程中分离挥发性化合物并降低压力的方法和设备

摘要

Oligomer deposits and monomer can be separated volatile condensable components of the vapor from the last stage of the melt phase polycondensation and generates the present invention relates vacuum, and reduces the steam capacity compared to prior art methods provide a method for avoiding the failure caused. [SOLUTION] The reactor to be vacuum, steam jet apparatus of one or more attached to the spray condenser to be located upstream or downstream thereof is connected at the suction side, this object is achieved when the It is solved by phenol-containing liquid or liquid phenol is used as a spray material phenol-containing vapor and is used or phenol with a pressure of about 1.5MPa 0.5hPa~ as drive steam.
机译:低聚物沉积物和单体可从熔融相缩聚的最后阶段中分离出蒸气的挥发性可冷凝组分,并产生与真空有关的本发明,并且与现有技术方法相比提供了减少蒸汽容量的方法,从而避免了引起故障的方法。 [解决方案]真空反应器,安装在喷雾冷凝器上游或下游的一个或多个蒸汽喷射装置连接在吸入侧,该目的是通过用含酚的液体或将其溶解来解决的。液态苯酚用作喷涂材料中含苯酚的蒸气,并用作压力约为1.5MPa 0.5hPa〜的苯酚作为驱动蒸汽。

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