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The high boiling point residue from direct method the high boiling point residue which is obtained from the haidorokurorineshiyon modulo null
The high boiling point residue from direct method the high boiling point residue which is obtained from the haidorokurorineshiyon modulo null
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机译:直接法制得的高沸点残渣是从haidorokurorineshiyon模取空得到的高沸点残渣
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摘要
PROBLEM TO BE SOLVED: To efficiently convert the subject high boiling point residue into a monosilane compound by brining hydrogen chloride into contact with the mixture of the high boiling point residue obtained by the reaction of an organic chloride with silicon metalloid with a silane compound in the presence of a catalyst composition. ;SOLUTION: This hydrochlorination method comprises mixing an organosilane compound of formula I [R is a 1-6C alkyl, an aryl, a 1-6C alkoxy, trimethylsily, trifluoropropyl; (m) is 1-4; (n) is 0-2; (m)+(n)=2 to 4] with a high boiling point residue obtained by the reaction of an organic chloride with silicon metalloid, and subsequently bringing the mixture into contact with hydrogen chloride in the presence of a catalytic amount of a catalyst composition effective for accelerating the formation of a monosilane compound from the high boiling residue at a temperature of 150-500°C and at a whole reactor gauge pressure of 689.5kPa to 34.5MPa (100-5000psi) to obtain the monosilane compound of formula II [(y) is 0-4; (n) is 0-3; (y)+(z)=0-4].;COPYRIGHT: (C)1998,JPO
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