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Lightweight boron carbide materials with improved mechanical properties and process for their manufacture
Lightweight boron carbide materials with improved mechanical properties and process for their manufacture
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机译:具有改善的机械性能和制造工艺的轻质碳化硼材料
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摘要
This disclosure describes sintered bodies comprising about 90 wt % to about 99 wt % of boron carbide, having a B:C atomic ratio ranging from 3.8 to 4.5:1; 0 to 1 wt % free carbon; 0 to 1 wt % BN or AlN, remainder an oxide binder phase; said sintered body having a uniform microstructure composed of substantially equiaxed grains of said boron carbide; the oxide binder phase comprising at least a rare earth aluminate and optionally Al2O3 or other ternary or binary phases of rare earth oxide-alumina systems; the binder phase being present in form of pockets at the multiple grain junctions and the density of no more than 2.6 g/cm3. Also described is a manufacturing process for the above described substantially pore-free, sintered boron carbide materials with high strength and fracture toughness, which can be used for production of large-area parts. This is achieved by liquid phase low temperature-low pressure hot pressing of boron carbide in an argon atmosphere.
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机译:该公开内容描述了一种烧结体,该烧结体包含约90wt%至约99wt%的碳化硼,其B∶C原子比为3.8至4.5∶1;优选地,所述B∶C的原子比为0.1。 0-1 wt%的游离碳; 0-1%(重量)的BN或AlN,其余为氧化物粘合剂相;所述烧结体具有均匀的微观结构,该组织由基本上等轴的所述碳化硼晶粒组成;氧化物粘合剂相至少包含稀土铝酸盐和任选的Al 2 Sub> O 3 Sub>或稀土氧化物-氧化铝体系的其他三元或二元相;粘结相以袋状存在于多个晶粒连接处,密度不超过2.6 g / cm 3 Sup>。还描述了用于上述具有高强度和断裂韧性的基本无孔的烧结碳化硼材料的制造方法,其可用于大面积零件的生产。这是通过在氩气氛中对碳化硼进行液相低温低压热压而实现的。
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