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REE IGNEOUS ROCK SCIENTIFIC EXTRACTION AND THE COMPOSITE

机译:稀土岩石科学提取及其复合材料

摘要

A method for preparing a mixture of rare-earth elements is provided to extract and separate rare earth elements from igneous rocks at a low cost, and to widen a physical property range of a useful component at a low energy cost. A method for preparing a mixture of rare-earth elements containing natural radioactive nuclei from granodiorite includes the steps of: grinding the granodiorite into powder(40 micron or smaller), mixing the powder with distilled water to obtain a saturated aqueous solution, dispersing the solid particles sufficiently using a homogenizer, and performing dispersion and breaking to obtain the saturated aqueous solution having a particle size of 10 micron or smaller; and cooling the saturated aqueous solution, sublimating water by a low-temperature drying method, dry-breaking the resultant to obtain recrystallized powder, re-saturating the fine powder with distilled water, stirring the re-saturated solution for 120 minutes or more using an ultrasonic homogenizer of 20 Kh, removing all water, adding diethylenetriaminepentaacetate to the resultant, sonicating the admixture to obtain a filtrate, centrifuging the filtrate to separate out SiO2 and clay, collecting floating particles, and performing a specific gravity sorting method and a wet magnetic force sorting method at the same time.
机译:提供一种制备稀土元素混合物的方法,以低成本从火成岩中提取和分离稀土元素,并以低能耗降低有用成分的物理性质范围。由花岗闪长岩制备含有天然放射性核的稀土元素混合物的方法包括以下步骤:将花岗闪长岩研磨成粉末(40微米或更小),将粉末与蒸馏水混合以获得饱和水溶液,将固体分散使用均化器充分地分散粒子,进行分散,破碎,从而得到粒径为10μm以下的饱和水溶液。冷却饱和水溶液,通过低温干燥法将水升华,将所得物干燥破碎以获得重结晶粉末,用蒸馏水使细粉末重新饱和,使用Na2SO3将该再饱和溶液搅拌120分钟以上。 20 Kh的超声均质机,除去所有水,向所得物中添加二乙撑三乙五胺二乙酸酯,将混合物超声处理以获得滤液,将滤液离心分离出SiO2和粘土,收集漂浮颗粒,并进行比重分选方法和湿磁力同时排序方法。

著录项

  • 公开/公告号KR20080093505A

    专利类型

  • 公开/公告日2008-10-22

    原文格式PDF

  • 申请/专利权人 YOON NAM DEOK;

    申请/专利号KR20070037264

  • 发明设计人 YOON NAM DEOK;

    申请日2007-04-17

  • 分类号C01F17;B01J23/10;B01J21/06;

  • 国家 KR

  • 入库时间 2022-08-21 19:52:51

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