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CLAY MODIFIED WITH SILANE COMPOUND, POLYMER/CLAY NANOCOMPOSITE CONTAINING THE CLAY COMPOUND, AND METHODS FOR PREPARING THEM

机译:硅烷化合物改性的粘土,包含该粘土化合物的聚合物/粘土纳米复合材料及其制备方法

摘要

A method for preparing a clay compound modified with a silane compound is provided to obtain a polymer/clay nanocomposite having excellent tensile modulus and tensile elongation while maintaining high transparency, and useful for elastic bodies for absorbing vibration and impact in various types of industrial machines. A method for preparing a clay compound modified with a silane compound comprises the steps of: (i) adding a silane compound to an aqueous solvent, and adding an acid thereto to perform hydrolysis; and (ii) adding clay to the hydrolyzed silane compound solution and agitating the mixture, followed by drying. In step (i), the aqueous solvent is a mixed solvent of ethanol/distilled water. The acid used in the step (i) is selected from the group consisting of phosphoric acid, acetic acid and formic acid.
机译:提供一种制备用硅烷化合物改性的粘土化合物的方法,以获得具有优异的拉伸模量和拉伸伸长率,同时保持高透明性,并且可用于吸收各种工业机械中的振动和冲击的弹性体的聚合物/粘土纳米复合材料。一种制备用硅烷化合物改性的粘土化合物的方法,包括以下步骤:(i)将硅烷化合物加入到水性溶剂中,并向其中加入酸进行水解; (ii)将粘土加入到水解的硅烷化合物溶液中并搅拌混合物,然后干燥。在步骤(i)中,水性溶剂是乙醇/蒸馏水的混合溶剂。步骤(i)中使用的酸选自磷酸,乙酸和甲酸。

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