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Reactor for producing organic peroxides via solid hydroperoxide intermediates

机译:通过固体氢过氧化物中间体生产有机过氧化物的反应器

摘要

A reactor which comprises a vessel (1) with a vessel bottom (2), a stirrer (3) arranged in the vessel, an emergency discharge valve (4) arranged in the vessel bottom for emptying the reactor in less than 600 seconds and at least one filtration device (5) arranged in the vessel bottom is suitable for the safe preparation of organic peroxides. The process for preparing an organic peroxide comprises the steps of preparing a solid hydroperoxide in the form of a suspension in the reactor, filtering the suspension through the filtration device (5) arranged in the vessel bottom (2) while retaining the solid hydroperoxide in the reactor and reacting the hydroperoxide with an alkylating agent, an acylating agent or a carbonyl compound.
机译:一种反应器,其包括具有容器底部(2)的容器(1),布置在容器中的搅拌器(3),布置在容器底部的紧急排放阀(4),用于在不到600秒的时间内将反应器排空布置在容器底部的至少一个过滤装置(5)适合安全地制备有机过氧化物。制备有机过氧化物的方法包括以下步骤:在反应器中制备呈悬浮液形式的固体氢过氧化物;通过布置在容器底部(2)中的过滤装置(5)过滤悬浮液,同时将固体氢过氧化物保留在容器中。使氢过氧化物与烷基化剂,酰化剂或羰基化合物反应。

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