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A PROCESS FOR THE PREPARATION OF DESGLUCODESRHAMNORUSCIN
A PROCESS FOR THE PREPARATION OF DESGLUCODESRHAMNORUSCIN
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机译:脱沙司沙门氏菌素的制备方法
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摘要
The present invention relate to a process for the preparing desglucodesrhamnoruscin, which comprises enzymatically hydrolyzing rhamnose-arabinose hetrosidic bond of Ruscus aculeatus steroid glycosides with crude hydrolase extracted from Aspergillus niger in aqueous solution at pH 5 or in water ethanol mixture containing up to 30% by volume of ethanol, at temperature from 20 to 40° C for times from 3 to 7 days by sequentional removal of (3-glucoside residue followed by removal of a-rhamnoside residue to provide a reaction mixture comprising the desglucodesrhamnoruscin which is recovered in a conventional manner.
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